BISCHOFF Chromatography - Peak Solutions

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Updated: 22.03.2009

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Dosing Pumps

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Dosing Pumps

HPD Multitherm 200
HPD Multitherm 200xl
HPLC Compact Pump 2250

HPD Multitherm 200

The new High Precision Dosing pump - model 2251 for normal and / or high temperature metering of fluids. The HPD Multitherm 200 covers a wide area of applications with it`s possibilities of variable flow ranges from micro to large flow (depending on the pump head), normal and / or high temperature and wide pressure range. As a high precision dosing pump it is a unique dosing unit for the use in microprocess technology and mini-plants where high pressure and and / or high temperature is needed.

Technical data:

Operation Temperature:	- 5 °C to + 200 °C
Pressure shut-off:	for P min and P max
Temperature shut-off:	if set temperature is exceeded
Compressibility:	adjustable
Flow rate accuracy:	better 3 %
Flow reproducibility:	better 0.5 %
Residual Pressure Pulsation:	better 3 %
Pump head identification:	automatically
Purge Key:	standard
External control:	by contact closures or active input by RS 232 or current loop all functions
Power requirements:	110/220 V +/- 10 % 50/60 Hz 50 VA
Dimensions:	381 x 255 x 130 mm (LxWxH)
Weight (without pumphead):	8.7 kg
P/N 2251 0000

Pump Heads:

· HT0	Flow : 0,001 - 0,999 ml/min pressure range: 0 - 60 MPa P/N 2251 0100
· HT1	Flow : 0,010- 4,99 ml/min pressure range: 0 - 50 MPa P/N 2251 0200
· HT2	Flow : 0,100-19,99 ml/min pressure range: 0 - 15 MPa P/N 2251 0300
· HT3	Flow 0,100-39,99 ml/min pressure range: 0 - 5 MPa P/N 2251 040

Options:

Pump Heads (on request)
· Titanium	Flow 0,01-4,99 ml/min pressure range: 0 - 50 MPa
· Hasteloy C	Flow 0,01-4,99 ml/min pressure range: 0 - 50 MPa
Analogue-Interface	for external control via current or voltage P/N 3.709.4000
Temperature Control Unit TCU 200	Including sensor cables. P/N 2251 2000
Thermo Jacket HT	Ambient to 200° C(for all pump heads) with integrated sensors (Temperature Control Unit needed) P/N 2251 1000
Thermo Jacket LT	Ambient to - 5° C(for all pump heads) (Refrigerated Circulator needed) P/N 2251 1010

Fig 1: Pump and Control Unit

Fig 2: HPD Pump with Thermo Jacket (for all pump heads)

Fig 3: Temperature Control Unit: TCU 200

HPD Multitherm 200 XL

MULTITHERM 200 XL the multipurpose pump for PREPARATIVE HPLC and HIGH PRECISION DOSING applications is designed for continuous operation under full workload. The compact design and its performance is a result of about 20 years in manufacturing and developing of HPLC and High Precision Dosing Pumps. The pump is a real dual piston pump with active pulse dampening controlled by software. The pump head is designed for a flow rate from 0.1 to 200 ml/min and a pressure range from 0 to 20 MPa. All parts in contact with the pumped solvents or solutions are made of stainless steel, PTFE, P TFE compound, sapphire and ceramics.

Specifications

Flow rate range	0.1 ml/min - 200 ml/min
Flow rate accuracy	+/- 2 % (within 2 – 50 % of flow range, measured with MeOH/H2O 80/20 v/v)
Flow reproducibility	0.2 %
Pressure range	0 MPa - 20 MPa
Pressure pulsation	electronic control of residual pulsation
Pressure shut-off	P min, P max , adjustable
Purge valve	manual
Display	2 x 24 digits
Input	by 16 push button keys
Programing	up to 20 methods, up to 10 queues
Remote control	via RS 232 all functions, remote start, flow rate Via analogue input
Gradient	High pressure gradient (binary or ternary, with additional pumps (master/slave configuration) Low pressure gradient (ternary, with valve system)
Auxiliary outputs	8 event outputs (TTL, OC, relays), pressure
Power requirements	115/230 V, 47 -63 Hz, 450 W
Dimensions	255 x 195 x 381 mm (W x H x D)
Weight	12 kg
Ordering information	P/N 22520000

HPLC Compact Pump 2250

Model 2250 - The serial dual piston pump for routine and research

Technical requirements and design

Current users of modern HPLC pumps expect to obtain not only minimum pulsation and a solvent independent flow reproducibility, but also an optimum performance over the largest possible ranges of flow and pressure combined with a high resistance against salt solutions in the pump head. Operation should be possible either in stand-alone mode or via a computer or a central processor.

A user-oriented design should allow easy handling and maintenance.

The model 2250 HPLC Compact Pump, manufactured under ISO 9001 satisfies all these requirements and is therefore suitable for use in both simple isocratic and gradient HPLC systems:

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The serial dual piston pump with only two check valves gurantees a minimum rest pulsation. The use of an additional pulse damper is generally not necessary even when using pulsationsensitive detectors such as Refractiv Index detector or Electrochemical detector.

Easily interchangeable pump heads cover a wide linear range of flow rates and allow operation with microbore, analytical, preparative and short columns for fast HPLC. Three different pump heads can be used for various application areas.

Electronic pump head identification with automatic control of flow and pressure ranges simplifies the use of the pump for the different applications.

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Typical flow ranges are:

Micro pump head
Flow range: 1 - 999 µL/min

Analytical pump head
Flow range: 10 - 4999 µL/min

Preparative pump head
Flow range: 1.0 - 19.99 mL/min

Pump head, stainless steel

The pump head includes the complete liquid delivery unit and is easily accessible for maintenance. Due to the serial arrangement of pistons and the use of only two check valves the model 2250 HPLC Compact Pump combines the advantages of a single piston pump with those of a dual piston pump.

For applications with buffers the pump head can be provided with a piston back wash assembly. Rinsing of high pressure piston seals prevents a possible crystallisation of buffer salts which might penetrate behind the seals through existing micro leakages, thereby causing damage to the seals. Thus, a wet or humid space behind the seal can prevent crystallisation.

Various check valve cartridges are available for different applications and for the analytical, microbore, and preparative flow range.

Service and Maintenance

Rear panel of the model 2250 HPLC Compact Pump

The model 2250 HPLC Compact Pump can be used for high pressure or low pressure gradients. To run a high pressure gradient you need one additional model 2250 HPLC Compact Pump and the model 1152 Central Processor for gradient control. In low pressure mode there is only the need for the model 1152 Central Processor and the model 1150 Low Pressure Gradientmixer which is available for binary or ternary gradients. Programming of both kinds of gradient modes is the same, there is no need to learn different program structures.

Micro piston/analytical piston

Flushing unit

Valve assemblies

The compact design simplifies maintenance because parts like the pump head are easily accessible. The pump can be upgraded to the latest software version by simply interchanging an EPROM on the main board inside the pump.

EPROMs for special applications, such as for slow start-up flow program for column protection are also available.

Specifications

Flow rate range	Pump head M Pump head A Pump head P	0.001 - 0.999 mL/min 0.01 - 4.99 mL/min 0.1 - 19.9 mL/min

Flow rate accuracy	at 20 - 80 % FS	£ 3 %
Flow reproducibility		£ 0.5 %
Pressure range	Pump head M Pump head A Pump head P	0 - 60 MPa 0 - 50 MPa 0 - 15 MPa
Pump head volumes (analytical) - main piston - priming piston		54 µL 20 µl
Pump displacement volumes - main piston - priming piston		45 µL 14 µl
Length of stroke - main piston - priming piston		5.6 mm 1.8 mm
Residual pressure pulsation at 2 mL/min and 20 MPa into a 125 mm column	compensated by setting the proper compressibility	£ 3 %
Pressure measurement	a) volume of the pressure transducer	50 µL
	b) accuracy	3 %
	c) resolution of the display	0.1 MPa
	d) recorder output	1 mV/MPa
Pressure shut down	a) maximum switch-off time b) minimum switch-off time alter initial delay of 2 min not effective at 0.0 MPa	adjustable 0 to FS £ 20 ms 0.1 to FS 3 cycles
Compressibility		adjustable
Correction mode		manually
Purge valve		standard
Purge key		runs maximum flow of installed head
Display alternatively	a) flow b) pressure c) compressibility	6 digit LED display with sign and pump head type other than standard
Pump head identification		automatically
Input		by 6 push button keys
External control	by contact closures or active input	a) stop pump b) reduce flow
	by RS 232 or current loop	all functions
Auxiliary outputs		a) suction phase b) pump stop
Power requirements		110/220 V ± 10% 50/60 Hz 50 VA
Temperature range		+15°C up to +30°C
Dimensions		381 x 255 x 133 mm
Weight		8.7 kg